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Variable temperature dewar for infrared absorption studies MacPherson, Ronald William
Abstract
A variable temperature dewar has been designed and built at the solid state laboratory of the University of British Columbia for infra-red absorption experiments at low temperatures. The dewar features a rotatable sample holder which brings any one of three samples into the light beam for comparison measurements. A removable tail section permits easy access to the samples.
The dewar has been successfully operated over the 4°K to 50°K range. It can maintain sample temperatures to within 1°K for periods up to two hours. Approximately ten minutes is required to achieve any desired temperature in the operating range.
The construction and calibration of a copper vs. constantan thermocouple is described. The thermocouple was used to measure the sample temperatures to an accuracy of about 1°K. Temperature variations of a few tenths of a degree could be detected.
As a demonstration of the dewar's capabilities, an experiment was performed to measure the line width dependence of hole transitions from the ground state of the P3/2 band to the first excited state in the P1/2 band in boron doped silicon. The experiment showed that the line broadening starts at about 20°K and increases at higher temperatures.
Several methods of improving the performance of the dewar are suggested.
Item Metadata
| Title |
Variable temperature dewar for infrared absorption studies
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| Creator | |
| Publisher |
University of British Columbia
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| Date Issued |
1965
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| Description |
A variable temperature dewar has been designed and built at the solid state laboratory of the University of British Columbia for infra-red absorption experiments at low temperatures. The dewar features a rotatable sample holder which brings any one of three samples into the light beam for comparison measurements. A removable tail section permits easy access to the samples.
The dewar has been successfully operated over the 4°K to 50°K range. It can maintain sample temperatures to within 1°K for periods up to two hours. Approximately ten minutes is required to achieve any desired temperature in the operating range.
The construction and calibration of a copper vs. constantan thermocouple is described. The thermocouple was used to measure the sample temperatures to an accuracy of about 1°K. Temperature variations of a few tenths of a degree could be detected.
As a demonstration of the dewar's capabilities, an experiment was performed to measure the line width dependence of hole transitions from the ground state of the P3/2 band to the first excited state in the P1/2 band in boron doped silicon. The experiment showed that the line broadening starts at about 20°K and increases at higher temperatures.
Several methods of improving the performance of the dewar are suggested.
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| Genre | |
| Type | |
| Language |
eng
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| Date Available |
2011-09-01
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| Provider |
Vancouver : University of British Columbia Library
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| Rights |
For non-commercial purposes only, such as research, private study and education. Additional conditions apply, see Terms of Use https://open.library.ubc.ca/terms_of_use.
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| DOI |
10.14288/1.0085912
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| URI | |
| Degree (Theses) | |
| Program (Theses) | |
| Affiliation | |
| Degree Grantor |
University of British Columbia
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| Campus | |
| Scholarly Level |
Graduate
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| Aggregated Source Repository |
DSpace
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Rights
For non-commercial purposes only, such as research, private study and education. Additional conditions apply, see Terms of Use https://open.library.ubc.ca/terms_of_use.