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He3 cryostat for steady state nuclear magnetic resonance measurements in metals Puls, Manfred Paul
Abstract
A He³ cryostat was designed for steady state nuclear magnetic resonance measurements. The cryostat required about one liter of He³ at NTP. This amount of He³ was liquified at 1.2°K, which was the temperature of the surrounding liquid He⁴ bath, and then pumped on by means of a four-stage mercury diffusion pump. By this procedure, a liquid He³ temperature of 0.35 K was achieved and maintained for four hours. The r-f coil and sample were in direct contact with the liquid He³ to ensure sufficient heat transfer between the two. The temperature of the liquid He³ was measured by means of vapour pressure measurements of the evaporating He³ and by means of resistance measurements of a carbon resistance in contact with the liquid He³. The system was non-recirculating, since a total, uninterrupted run of four hours was considered long enough for most experiments. The He³ could also be retransferred within 20 minutes after such a run, and this process could be continued until in-sufficient quantities of liquid He⁴remained to cool the surroundings.
Item Metadata
Title |
He3 cryostat for steady state nuclear magnetic resonance measurements in metals
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Creator | |
Publisher |
University of British Columbia
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Date Issued |
1966
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Description |
A He³ cryostat was designed for steady state nuclear magnetic resonance measurements. The cryostat required about one liter of He³ at NTP. This amount of He³ was liquified at 1.2°K, which was the temperature of the surrounding liquid He⁴ bath, and then pumped on by means of a four-stage mercury diffusion pump. By this procedure, a liquid He³ temperature of 0.35 K was achieved and maintained for four hours. The r-f coil and sample were in direct contact with the liquid He³ to ensure sufficient heat transfer between the two. The temperature of the liquid He³ was measured by means of vapour pressure measurements of the evaporating He³ and by means of resistance measurements of a carbon resistance in contact with the liquid He³. The system was non-recirculating, since a total, uninterrupted run of four hours was considered long enough for most experiments. The He³ could also be retransferred within 20 minutes after such a run, and this process could be continued until in-sufficient quantities of liquid He⁴remained to cool the surroundings.
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Genre | |
Type | |
Language |
eng
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Date Available |
2011-10-06
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Provider |
Vancouver : University of British Columbia Library
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Rights |
For non-commercial purposes only, such as research, private study and education. Additional conditions apply, see Terms of Use https://open.library.ubc.ca/terms_of_use.
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DOI |
10.14288/1.0085814
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URI | |
Degree | |
Program | |
Affiliation | |
Degree Grantor |
University of British Columbia
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Campus | |
Scholarly Level |
Graduate
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Aggregated Source Repository |
DSpace
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Rights
For non-commercial purposes only, such as research, private study and education. Additional conditions apply, see Terms of Use https://open.library.ubc.ca/terms_of_use.