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The transition from stress corrosion cracking to corrosion fatigue in AA-7075 and AA-8090

University of British Columbia

The effect of crack tip strain rate (CTSR) on environmentally assisted cracking was studied for alloys AA-7075 (Al-Zn-Mg-Cu) and AA-8090 (Al-Li-Cu-Mg) in the artificially aged condition. Fatigue pre-cracked double cantilever beam (DCB) specimen were employed with the crack plane parallel to the rolling plane. The cracking behaviour under monotonic and cyclic loading conditions was investigated in aqueous sodium chloride solutions with and without additions of sodium chromate as a corrosion mhibitor. CTSR values were described in terms of K-rate ∆K/∆t (ie. dK/dt) as a measured average over the loading period of a fatigue cycle. This allowed a comparison with CTSR's of monotonically increasing load or constant load tests. At frequencies ≤1 Hz, the load was applied with a triangular wave form. A high frequency of 30 Hz was obtained by sinusoidal loading. Expressed as K-rate, CTSR values were varied over 7 orders of magnitude from 10⁵MPa√m/s to 10² MPa√m/s. Stress intensities investigated were mainly around region II values with respect to SCC K-log(da/dt) behaviour. At low K-rates, real time crack velocities (da/dt) measured under monotonic slow loading or constant load conditions were comparable to crack velocities obtained with cyclic loading experiments. As the K-rate was increased from low values, typical of constant load experiments, the real time crack velocities decreased. This was caused by plasticity induced crack growth retardation effects and a decrease in crack tip film rupture events during the unloading part of a cycle. The crack propagation rate decreased until minimal crack advance increments per cycle were dictated by mechanical parameters acting on a hydrogen embrittled crack tip region. Under monotonic loading conditions region II crack velocities were not influenced by an increase in K-rate which was explained with a mass transport controlled cracking process. Tests with alloy 7075 at intermediate K-rates and a high R-ratio of 0.78 allowed a crack tunnelling mechanism to operate. This overcame the plasticity induced crack growth retardation and, therefore, cracks propagated at the same rates as during low K-rate tests where no retardation phenomena were encountered. Scanning electron microscope investigations revealed a striated intergranular fracture surface of alloy 7075 if tested at K-rates above the transition value to K-rate independent crack propagation rates. Individual striations could be matched on opposing fracture surfaces and the striation spacing corresponded to the average crack propagation increment per cycle. The striations, therefore, were formed as part of the crack advance during every fatigue cycle. At the lower K-rates no striations were present but micro tear ridges could be found on the intergranular fracture facets indicating that dissolution processes alone did not cause the intergranular crack advance. Alloy 8090 did not reveal significant changes in fractography over the entire K-rate range investigated, except at the highest K-rates where small interlocking steps could be detected on some opposing transgranular fracture surfaces. In general, however, the crack path at all K-rates was mainly intergranular with dimpled fracture facets. Alloy 8090 exhibited a high resistance to SCC with fatigue pre-cracked DCB specimen. Therefore, to obtain crack velocity values with low K-rate monotonic loading tests very long test durations would have been necessary. It is concluded that the transition from intergranular SCC to intergranular CF occurs at a critical K-rate. Below the critical K-rate crack velocities are not increased by cyclic loading. Instead crack growth retardation effects can result in lower real time crack velocities than those typical for constant load tests at comparable stress intensities but much lower K-rates.

Text

2011-01-24

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http://hdl.handle.net/2429/30779

Materials Engineering

University of British Columbia

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