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UBC Theses and Dissertations
Synthetic modifications of guest host properties in calix[6]arenes Vandel, Mason Sheldon
Abstract
This project investigated the synthesis and characterization of several calix[6]arene azo dyes and attempts to link calix[6]arenes with terpyridine moieties with various alkyl chains. Mass spectrometry was used to confirm the presence of the fully substituted dyes as well as several partially substituted calix[6]arenes. ¹H NMR spectroscopy was used to propose a possible conformation of one of the calix[6]arene dyes as well as characterize several allyl substituted calix[6]arenes. NMR studies were also used to identify the product of a Mitsunobu cross coupling reaction between calix[6]arene and terpyridine.
Item Metadata
Title |
Synthetic modifications of guest host properties in calix[6]arenes
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Creator | |
Publisher |
University of British Columbia
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Date Issued |
2013
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Description |
This project investigated the synthesis and characterization of several calix[6]arene azo dyes and attempts to link calix[6]arenes with terpyridine moieties with various alkyl chains. Mass spectrometry was used to confirm the presence of the fully substituted dyes as well as several partially substituted calix[6]arenes. ¹H NMR spectroscopy was used to propose a possible conformation of one of the calix[6]arene dyes as well as characterize several allyl substituted calix[6]arenes. NMR studies were also used to identify the product of a Mitsunobu cross coupling reaction between calix[6]arene and terpyridine.
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Genre | |
Type | |
Language |
eng
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Date Available |
2013-04-17
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Provider |
Vancouver : University of British Columbia Library
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Rights |
Attribution-NonCommercial-NoDerivatives 4.0 International
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DOI |
10.14288/1.0073791
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URI | |
Degree | |
Program | |
Affiliation | |
Degree Grantor |
University of British Columbia
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Graduation Date |
2013-05
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Campus | |
Scholarly Level |
Graduate
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Rights URI | |
Aggregated Source Repository |
DSpace
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Item Citations and Data
Rights
Attribution-NonCommercial-NoDerivatives 4.0 International